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After HPLC separation and electronspray ionization mass spectrometric analyses (HPLC-ESI/MS) were performed with an HPLC MS system (Shimadzu, Japan) comprising two LC-20 AD high pressure liquid-delivery units, a SIL-20AC HT autosampler, a CTO-20A column thermostat, an SPD-M20A UV/VIS photodiode array detector, and an LCMS 2020 single quadrupole mass spectrometer equipped with an ESI sample pulverization unit

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