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Renal effects, including acute kidney injury, have been reported rarely in post-marketing surveillance, typically in the context of severe gastrointestinal adverse effects leading to dehydration

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After the reaction was completed, a blocking solution consisting of 45 ml methanol and 15 ml DIPEA was added into the reaction column for another 30 min

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The target peak retention time was then used to calculate (using CEM Focused Gradient Calculator software, version 1.1.673.1159) optimized focused gradients for each purification